Analysis – Page 18
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Research
Frozen fluorine’s structure revisited after 50 years
Second ever crystal structure of solid fluorine solves 50-year-old crystal symmetry conundrum
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Co-crystals fish out cannabinoid from plant extract
Purifying cannabidiol from natural cannabis extract made cheap and easy thanks to amino acid partner
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Machine learning predicts ammunition from gunshot residue
Forensic tool will assist investigators by turning back time on firearm chemistry
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Research
Synthesis-searching software’s superior scoring sharpens selections
Realistic costs and diverse suggestions make Chematica more insightful
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Research
'Self-destructing' solvents control crystallisation
‘Deep eutomic’ mixtures allow easy access to unusual pharmaceutical polymorphs
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The protein crystallisation influencer
Naomi Chayen discusses her career manipulating phase diagrams to produce high-quality protein crystals
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Research
Chameleon compounds from the cocrystal continuum
Indecisive crystals exploited to find new thermochromic materials
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App quantifies chemicals in thin layer chromatography
Most basic analytical procedure gets a smartphone makeover for quantitative measurements
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Research
Light pulse peels crystal layers off parent
Partial cis–trans isomerisation in photoactive organic molecule results in controlled fragmentation
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Research
Chemical analysis reveals origin of Pompeian mosaic tiles
Work will help to preserve ancient murals
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Molecular movie reveals how twisting methyl disturbs aspirin electrons
Femtosecond x-ray experiments show how small vibrations kick off electron redistribution around an entire aspirin molecule
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Mechanochemical simulations surprise with crystals behaving like putty
Inaugural picture of what happens when materials are bashed together reveals unexpected level of molecular transfer
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Study challenges hydrogen-ordered ice hypothesis
Scientists debate whether endotherm indicates a new phase of ice or a deep glassy state
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UV can introduce oxidation artefacts during protein purity tests
HPLC–UV–MS blamed for impurities spotted by AstraZeneca team
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Hunting for isotopes with EELS
Electron microscopy detects isotopically labelled molecules with nanoscale resolution
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Droplets retain crystal-like structure while sliding on vertical substrate
Surprising properties of soft material may have significant impact on polymer physics
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Patent-busting AI tool navigates around protected drug pathways
Organic retrosynthesis software can identify key bonds involved in patented reactions to find alternative pathways
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Research
Blue teeth reveal medieval nun's artistic talent
Analysis identifies traces of the precious stone lapis lazuli
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Research
Pore-forming toxins detect long strands of DNA
Lithium electrolyte helps aerolysin overcome electrostatic obstacle to detect ssDNA longer than 100 nucleotides
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Research
Metal-bound hydrogen atom with extreme NMR shift discovered
Hydrogen atom bound directly to iron detected at ultra-low shift by paramagnetic nuclear magnetic resonance for the first time